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L00423 2,4,6-Trimethylbenzyl chloride, 98%

CAS-Nummer
1585-16-6
Synonyme
alpha(2)-Chloroisodurene

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2,4,6-Trimethylbenzyl chloride, 98%

MDL
MFCD00000901
EINECS
216-440-3

Chemische Eigenschaften

Formel
C10H13Cl
Molmasse
168.67
Schmelzpunkt
37-42°
Siedepunkt
114-115°/10mm
Flammpunkt
106°(222°F)
Storage & Sensitivity
Keep Cold.

Literaturverweise

Carboxyl groups can be protected as their 2,4,6-trimethylbenzyl esters by reaction in DMF in the presence of triethylamine. The group can be cleaved by acidolysis (TFA or HBr in AcOH) or hydrogenolysis: Aust. J. Chem., 21, 2831 (1968).

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Also reported for the protection of thiols (cysteine), stable to refluxing TFA, unlike 4-methoxybenzyl, but cleavable with HF or TfOH-TFA: Coll. Czech. Chem. Commun., 46, 286 (1981), or Ag(I): Chem. Pharm. Bull., 38, 1551 (1990).

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GHS Gefahren- und Sicherheitshinweise

Gefahrenhinweise (EU): H314-H318

Causes severe skin burns and eye damage. Causes serious eye damage.

Sicherheitshinweise: P280-P305+P351+P338-P309-P310a

Wear protective gloves/protective clothing/eye protection/face protection. IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. IF exposed or if you feel unwell: Immediately call a POISON CENTER/doctor

Weitere Referenzen

Beilstein
386678
Gefahrenklasse
8
Verpackungsgruppe
II
Harmonized Tariff Code
2903.99
TSCA
No

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