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A convenient method for the direct ɑ-methylenation of ketones involving reaction with formaldehede, in the presence of N-Methylanilinium trifluoroacetate, A17781, is illustrated for this ketone: Org. Synth. Coll., 7, 332 (1990)./n
Reacts with arenes under Friedel-Crafts conditions to give 6-aryl-1-tetralones: J. Org. Chem., 55, 4036 (1990)./n
The use of the selective reduction system in liquid ammonia is illustrated by the clean reduction of 1-tetralone to the alcohol without over-reduction to tetralin or reduction of the aromatic ring: J. Org. Chem., 61, 1493 (1996)./n
Hazard Statements: H302-H331
Harmful if swallowed. Toxic if inhaled.
Precautionary Statements: P261-P264b-P270-P271-P301+P312-P304+P340-P311-P330-P501c
Avoid breathing dust/fume/gas/mist/vapours/spray. Wash face, hands and any exposed skin thoroughly after handling Do not eat, drink or smoke when using this product. Use only outdoors or in a well-ventilated area. IF SWALLOWED: Call a POISON CENTER or doctor/physician if you feel unwell. IF INHALED: Remove to fresh air and keep at rest in a position comfortable for breathing. Call a POISON CENTER or doctor/physician. Rinse mouth. Dispose of contents/ container to an approved waste disposal plant