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In Room temperature phosphorescence of α-bromonaphthalene induced by cyclodextrin in the presence of hexahydropyridine or 1-ethylpiperidine and its application is described. The highest yields of 5-Bromopyrimidine (37%) were obtained by using 1-ethylpiperidine or triethylamine as condensing agent. Tributyltin hydride and 1-ethylpiperidine hypophosphite were mediated intermolecular radical additions to 2, 4, 6-trichlorophenyl vinyl sulfonate.
G. E. Boxer,; P. M. Everett. Colorimetric Determination of Benzylpenicillin. Anal. Chem., 1949, 21 (6), 670-673.
J. F. W. McOmie,; I. M. White .623. Pyrimidines. Part VI. 5-Bromopyrimidine. J. Chem. Soc. 1953, volume 3129-3131.
Hindered, non-nucleophilic base. Preferred base for enantioselective crossed aldol condensations of Sn enolates: Tetrahedron, 40, 1381 (1984). Also found to give excellent results in the formation of anhydrides using Bis(2-oxo-3-oxazolidinyl)phosphinic chloride, L08775: Synthesis, 616 (1981). Has been used in peptide synthesis via pivaloyl mixed anhydrides: Coll. Czech. Chem. Commun., 27, 1273 (1962).
Hazard Statements: H225-H314-H318
Highly flammable liquid and vapour. Causes severe skin burns and eye damage. Causes serious eye damage.
Precautionary Statements: P260u-P201-P280a-P304+P340-P405-P501a
Obtain special instructions before use. Wear protective gloves and eye/face protection. IF INHALED: Remove to fresh air and keep at rest in a position comfortable for breathing. Store locked up. Dispose of contents/container in accordance with local/regional/national/international regulations.