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Dodecanonitrile in xylene is used as a solvent and in the presence of sulfur was reduced with molybdenum sulfide catalyst yielded 70-5% dodecylmercaptan.
Itabashi Kunio . Pressure-hydrogenation of Organic Compounds by Molybdenum Sulfide Catalyst. XI:Synthesis of Dodecyl mercaptan from Dodecanonitrile . J. Synth. Org. Chem. Jpn. . 1961, 19 (8), 597-601.
Louis B. Bjostad,; Wendell L. Roelofs. Sex pheromone biosynthesis in the red-banded leafroller moth, studied by mass-labeling with stable isotopes and analysis with mass spectrometry. Journal of Chemical Ecology. 1986, 12 2, 431-450.
Hazard Statements: H302-H312-H332
Harmful if swallowed. Harmful in contact with skin. Harmful if inhaled.
Precautionary Statements: P261-P264b-P270-P271-P280-P301+P312-P302+P352-P304+P340-P312-P330-P363-P501c
Avoid breathing dust/fume/gas/mist/vapours/spray. Wash face, hands and any exposed skin thoroughly after handling Do not eat, drink or smoke when using this product. Use only outdoors or in a well-ventilated area. Wear protective gloves/protective clothing/eye protection/face protection. IF SWALLOWED: Call a POISON CENTER or doctor/physician if you feel unwell. IF ON SKIN: Wash with plenty of soap and water. IF INHALED: Remove to fresh air and keep at rest in a position comfortable for breathing. Rinse mouth. Wash contaminated clothing before reuse. Dispose of contents/ container to an approved waste disposal plant