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In order to synthesize macrocycles containing pyridine, 2,6-his-(bromomethyl)pyridine was prepared by bromonating 2,6-di (hydroxymethyl)pyridine.
Wu Xinyan,; He Yongbin,; Wu Chengtai. New method for reducing 2, 6-pyridinedicarboxylic acid diethyl ester to 2, 6-di(hydroxymethyl) pyridine. Wuhan University Journal of Natural Sciences. 1996, 1 (1), 105-106.
Gielen. M.; Mohammed Bouala,; Bieseman M.; Mahieu B.,; Willem R. Diorganotin derivatives of 2,6-dihydroxymethylpyridine and of 3-5N-pyrrolidino)-1,2-propanediaol : synthesis, characterization and in vitro antitumor activity. Journal name. 1992, 34(3),549-559 .
Hazard Statements: H315-H319-H335
Causes skin irritation. Causes serious eye irritation. May cause respiratory irritation.
Precautionary Statements: P261-P280a-P305+P351+P338-P304+P340-P405-P501a
Avoid breathing dust/fume/gas/mist/vapours/spray. Wear protective gloves and eye/face protection. IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. IF INHALED: Remove to fresh air and keep at rest in a position comfortable for breathing. Store locked up. Dispose of contents/container in accordance with local/regional/national/international regulations.