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In the resolution system of (RS)-1-cyclohexylethylamine (CHEA) with (S)-mandelic acid (MA), the DCR (dielectrically controlled resolution) phenomenon was clearly observed.
Bingzhi Shi,; Tanjore K Narayanan,; Zhi-Ying Yang,; Bradley T Christian,; Jogeshwar Mukherjee. Radiosynthesis and in vitro evaluation of 2-(N-alkyl-N-1?-11C-propyl)amino-5-hydroxytetralin analogs as high affinity agonists for dopamine D-2 receptors. Nuclear Medicine and Biology. 1999, 26 (7),725-735.
Beverly A Clement,; Christina M Goff,; T.David A Forbes. Toxic amines and alkaloids from acacia rigidula Phytochemistry. 1998, 49 (5),1377-1380.
Kenichi Sakaia,; Rumiko Sakuraia,; Noriaki Hirayama. Molecular mechanism of DCR phenomenon observed in (RS)-1-cyclohexylethylamine-mandelic acid resolution system. Tetrahedron: Asymmetry. 2006, 17 (12),1812-1816.
Hazard Statements: H314-H335
Causes severe skin burns and eye damage. May cause respiratory irritation.
Precautionary Statements: P260-P264b-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P363-P501c
Do not breathe dust/fume/gas/mist/vapours/spray. Wash face, hands and any exposed skin thoroughly after handling Use only outdoors or in a well-ventilated area. Wear protective gloves/protective clothing/eye protection/face protection. IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower. IF INHALED: Remove to fresh air and keep at rest in a position comfortable for breathing. IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER or doctor/physician. Wash contaminated clothing before reuse. Dispose of contents/ container to an approved waste disposal plant