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Lithium aluminum di-n-butylamide is used as a reagent for the determination of hydroxyl groups in silanols.
Reagent for determination of silanols: Anal. Chem., 39, 1623 (1967); Analysis of Silicones, A. L. Smith, Ed., Wiley, N.Y. (1974).
Kozlova, S. A.; Kirik, S. D. Post-synthetic activation of silanol covering in the mesostructured silicate materials ???-41 and SBA-15. Microporous Mesoporous Mater. 2010, 133, (1), 124-133.
Kosonen, J. P.; Ruohonen, J. K. A Simple Karl Fischer Titration Procedure for Determination of Total Hydroxyl Content in Silanol-Terminated Polvsiloxanes. Int. J. Polym. Anal. Charact. 1998, 4 (4), 283-293.
Hazard Statements: H226-H333-H315-H319
Flammable liquid and vapour. May be harmful if inhaled. Causes skin irritation. Causes serious eye irritation.
Precautionary Statements: P210-P280a-P280a-P303+P361+P353-P305+P351+P338-P501a
Keep away from heat/sparks/open flames/hot surfaces. - No smoking. Wear protective gloves and eye/face protection. IF ON SKIN (or hair): Remove/Take off immediately all contaminated clothing. Rinse skin with water/shower. IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Dispose of contents/container in accordance with local/regional/national/international regulations.