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583-68-6 - 2-Bromo-4-methylaniline, 99% - 4-Amino-3-bromotoluene - 2-Bromo-p-toluidine - A13818 - Alfa Aesar

A13818 2-Bromo-4-methylaniline, 99%

CAS 번호
583-68-6
동의어
4-Amino-3-bromotoluene
2-Bromo-p-toluidine

사이즈 가격 ($) 수량 재고 여부
10g 36.90
50g 137.00
250g 600.00
장바구니에 추가 대량 견적에 추가 항목 보기

2-Bromo-4-methylaniline, 99%

MDL
MFCD00007635
EINECS
209-515-7

화학적 특성

화학식
C7H8BrN
화학 식량
186.06
융점
14-16°
비등점
240-242°
인화점
>110°(230°F)
밀도
1.494
굴절률
1.6030
용해도
Insoluble in water.

용도

The N-(3, 5-Dichlorophenyl) naphthaldimine was obtained from the reaction of 2-hy- droxynaphthalene-l-carbaldehyde (0.01 mol) with a solution of 2-bromo-4-methylaniline (0.01 mol) in 40 ml of ethanol. Reaction of 2-bromo-4-methylaniline was quite clean, albeit 3,4-diaminotoluene was isolated just in 37% yield after flash chromatography on silica gel. The bromomethylquinoline starting material 16 was synthesized in two steps using an optimized process route by condensing 2-bromo-4-methylaniline.

참고

Store in cool place. Keep container tightly closed in a dry and well-ventilated place. Store away from strong oxidizing agents.

참조 문헌

Renee Aspiotis,; Denis Deschênes,; Daniel Dubé,; Yves Girard,; Zheng Huang,; France Laliberté,; Susana Liu,; Robert Papp,; Donald W. Nicholson,; Robert N. Young.The discovery and synthesis of highly potent subtype selective phosphodiesterase 4D inhibitors. Bioorganic & Medicinal Chemistry Letters 2010, 20(18), 5502-5505.

A. Elmali,; Y. Elerman,; I. Svoboda and H. Fuess. N-(3,5-Dichlorophenyl)naphthaldimine. Acta Cryst.. 1998, c54 974-976.

GHS 해저드 및 주의 설명서

해저드 설명서 (EU): H301-H311-H315-H319

Toxic if swallowed. Toxic in contact with skin. Causes skin irritation. Causes serious eye irritation.

주의 설명서: P280h-P305+P351+P338-P309-P310a-P302+P352a

Wear protective gloves/clothing. IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. IF exposed or if you feel unwell: Immediately call a POISON CENTER/doctor IF ON SKIN: Wash with plenty of water.

기타 참조

바일슈타인
1931711
위험 등급
6.1
포장 그룹
III
통합 관세 코드
2921.43
TSCA(독성물질규제법)"
Yes
RTECS(화학물질 독성 등록)
XU4300000

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